Newton: pendulum tests (@ 1 part in 103 )
But this was about 80 years after Galileo’s first experiments…
Newton
•Newton major contribution (beyond UFF ® equivalence)
Principia, (Definition I) : “this quantity that I mean hereafter under the name of ...mass ...is known by the weight ...for it is proportional to the weight as I have found by experiments on pendulums, very accurately made...”   
•Pendulum tests later improved to @ 1 part in 105 (Bessel….)